U.S. Department of Agriculture: Animal and Plant Health Inspection Service

 

United States Department of Agriculture Wildlife Services: Staff Publications

Document Type

Article

Date of this Version

1997

Citation

Journal of Chromatographic Science, Vol. 35, September 1997

Abstract

A gas chromatographic method for the analysis of nine organochlorine pesticides in wildlife urine is described. Reversedphase solid-phase extraction is utilized to extract the organochlorine pesticides from urine. The pesticides are recovered by elution with hexane-ethyl ether (1:1) and quantified by gas chromatography with electron-capture detection. Method detection limits range from 1.4 to 2.7 μg/L. Mean recoveries for all pesticides are 90.6%.

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