Mechanical & Materials Engineering, Department of

 

Date of this Version

2009

Comments

Published in Microsc Microanal 15(Suppl 2), 2009. Copyright 2009 Microscopy Society of America. Used by permission.

Abstract

To investigate the self-assembled growth of organosilane molecules carrying Si, C and H to form multiple layers, samples were prepared in toluene and then transferred to TEM Cu grids coated with thin C films for TEM observation. It is surprising that micrometer sized flakes with a main composition of Mg and Si (or Al and Si) were occasionally observed in the TEM specimens, later were identified as lizardite-1T phase. To trace down the source of the inorganic particles, all procedures in the sample preparation were carefully checked. The particles of the lizardite-1T phase were confirmed from the organic solvent of toluene.

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